n this work, The Reduced Graphene oxide (RGO) was prepared from the pure Graphite powder by using modified Hummer’s method. The synthesized RGO was characterized through X-ray diffraction (XRD), Fourier transform infra-red spectroscopy(FTIR), Micro-Raman, Scanning electron microscopy(SEM), high resolution transmission electron microscopy(HRTEM) with EDX and Cyclic Voltammetric studies. The XRD characteristic peak of graphene oxide (GO) appeared at 11.89˚ and the RGO characteristic peak spotted at 24.06˚. The functional group analysis of RGO was carried out by FTIR spectroscopy. The Raman characteristic peak of RGO appeared at 1338 cm-1and 1590 cm-1 which implies that the D band and G band of Sp2 carbon material. The SEM and HRTEM images of GO and RGO appeared as a layered nanosheet shapes. The EDX spectrum of RGO shows only carbon and oxygen element which indicates the purity of the RGO. The CV results of the RGO electrode exhibit a typical rectangular shape with good specific capacitance valueof 94 Fg-1@10 mvS-1

Reduced Graphene Oxide; SEM;HRTEM; Cyclic Voltammetric