Volume 19 No 6 (2021)
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The Debye Method is Used to Create 3D Structure Models of Electroactively Transformed Microcrystalline Cellulose
Ali M. Ahmed, Qasim Shakir Kadhim , Ibrahim A. Ali
Abstract
In this paper, we carried out the XRD results and 3D structural models of short-range order of amorphous cellulose obtained by ball milling of microcrystalline cellulose. The amorphous cellulose has the well-reproducible effect of influence of ozone treatment on its proton conductivity, which allows to use this material as a gas sensor. Calculation of the quantitative characteristics of the short-range order (radii of coordination spheres and their dispersions, coordination numbers) of amorphous cellulose was carried out from distribution pair functions curve by using the Finback-Warren method. The space atoms configurations was carried out by Debye method. After that, the models were distorted by converting into packages disoriented relative to each other layers. The X-Ray diffraction patterns were calculated for 3D models and compared with experimental curves.
Keywords
Microcrystalline Cellulose, Amorphous Cellulose, XRD Methods, 3D Structural Models, Finback-Warren Method, Debye Method.
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