XRD and Microscopic Images for Synthesis Graphite Nanoparticles by Oxidation Method

Volume 19 No 2 (2021)

Firas H. Abdulrazzak , Rawnaq B. Jimaa , Israa M. Radhi , Takialdin A. Himdan

DOI: 10.14704/nq.2021.19.2.NQ21016

Abstract

Graphite nanoparticles were successfully synthesized using mixture of H2O2/NH4OH with three steps of oxidation. The process of oxidations were analysis by XRD and optics microscopic images which shows clear change in particle size of graphite after every steps of oxidation. The method depend on treatments the graphite with H2O2 in two steps than complete the last steps by reacting with H2O2/NH4OH with equal quantities. The process did not reduces the several sheets for graphite but dispersion the aggregates of multi-sheets carbon when removed the Van Der Waals forces through the oxidation process

Keywords

Graphite, XRD, Nanoparticle, H2O2/NH4OH

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