A novel combination of materials are proposed for development of the cathode material. Through the research paper we are proposing synthesis of Lithium Manganese Oxide (LiMn2O4) material using hydrothermal process. In these assumptions, the time is kept constant and temperature is varied from 1200C to 1800C. The cathode element designed using novel combination is synthesized for lithium-ion batteries. Further, different ascendency parameters like Grain Size, Morphology, Electro Chemical properties are critically observed by varying temperature by Hydrothermal Synthesis process. Additionally, the XRD, SEM and TGA techniques are preferred for characterization purpose. Finally, the electrochemical analysis is carried out to understand the performance of the prepared cathode material

Rechargeable Battery, Discharge Control, Lithium-Ion, LiMn2O4, XRD, SEM, TGA